Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
DL-Phenylalanine, methyl ester → (R)-Methyl 2-amino-3-phenylpropanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | DL-Phenylalanine, methyl ester | HCID 75737 | — |
| 반응물 | N-(Benzyloxycarbonyl)-L-aspartyl-L-phenylalanine methyl ester | HCID 10159630 | — |
| 생성물 | (R)-Methyl 2-amino-3-phenylpropanoate | HCID 853474 | 62.3% |
반응 단계
Example 17 was repeated except for using DL-phenylalanine methyl ester instead of L-phenylalanine methyl ester to obtain 756 mg of an addition compound of N-benzyloxycarbonyl-L-aspartyl L-phenylalanine methyl ester and D-phenyl alanine methyl ester (1:1) (melting point: 105 to 111° C; yield: 62.3% based on N-benzyloxycarbonyl L-aspartic acid).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04165311 |
| 출처 데이터셋 | uspto-grants-1979_08 |
| ORD ID | ord-830efca480624c2d84a62dcda9023651 |
| 출처 메모 | uspto-grants-1979_08 |