Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → HCID 178511480, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | Hydroxyamine hydrochloride | HCID 443297 | — |
| 반응물 | 2-(4-Chlorobenzenesulfonyl)acetonitrile | HCID 735829 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178511480 | HCID 178511480 | 70% |
반응 단계
50 g. (0.23 mole) of 4-chlorophenylsulfonylacetonitrile were dissolved in 1.5 liters of ethanol and 16 g. (0.23 mole) of hydroxylamine HCl in 150 ml. of water was added to this solution, followed by the addition of 14.4 g. (0.12 mole) of Na2CO3 in 150 ml. of water. This reaction mixture was stirred at room temperature overnight. 58 g. crude product were filtered off; this was recrystallized from about 2.5 liters of ethanol to give 40 g. of the product (70% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04148801 |
| 출처 데이터셋 | uspto-grants-1979_04 |
| ORD ID | ord-cfb04106ce044c1b82b83425a88a2633 |
| 출처 메모 | uspto-grants-1979_04 |