Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 1,3-Bis-(4-carbomethoxy-2,6-dichlorophenoxymethyl)-2,4,5,6-tetrabromobenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | 2-Methoxyethanol | HCID 8019 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Methyl 3,5-dichloro-4-hydroxybenzoate | HCID 76856 | — |
| 반응물 | 1,2,3,5-Tetrabromo-4,6-bis(bromomethyl)benzene | HCID 14419177 | — |
| 생성물 | 1,3-Bis-(4-carbomethoxy-2,6-dichlorophenoxymethyl)-2,4,5,6-tetrabromobenzene | HCID 20571322 | — |
반응 단계
In a four-liter reaction vessel, 3 liters of methyl glycol (B.P. 122°-126° C.), 221 g (1 mole) of 3,5-dichloro-4-hydroxybenzoic acid methyl ester, 40 g (1 mole) of sodium hydroxide in 40 ml of water, and 289.8 g (0.5 mole) of 1,3-bis-(bromomethyl)-2,4,5,6-tetrabromobenzene were reacted and worked up in the manner described in Example 46.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04152511 |
| 출처 데이터셋 | uspto-grants-1979_05 |
| ORD ID | ord-e26386e68cc4414b80148d386f0c134c |
| 출처 메모 | uspto-grants-1979_05 |