rac-(1R,2R)-2-phenylcyclopentan-1-amine hydrochloride → N-[(1R,2S)-2-phenylcyclopentyl]azepan-2-imine;hydrochloride

HRID 261995

반응식

HRID 261995 반응식
[ClH:1].[C:2]1([C@H:8]2[CH2:12][CH2:11][CH2:10][C@H:9]2[NH2:13])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl.[C:15]1([C@@H:21]2CCC[C@H:22]2[NH2:26])[CH:20]=[CH:19][CH:18]=CC=1>>[ClH:1].[C:2]1([C@@H:8]2[CH2:12][CH2:11][CH2:10][C@H:9]2[N:13]=[C:22]2[CH2:21][CH2:15][CH2:20][CH2:19][CH2:18][NH:26]2)[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 70051154rac-(1R,2R)-2-phenylcyclopentan-1-amine hydrochlorideHCID 70053696trans-2-Phenylcyclopentan-1-amine hydrochloride

생성물 1

HCID 145795654N-[(1R,2S)-2-phenylcyclopentyl]azepan-2-imine;hydrochloride

실험 절차

Following the procedure of Example 1, only substituting for cis-2-phenylcyclopentylamine hydrochloride the appropriate molar equivalent amount of trans-2-phenylcyclopentylamine hydrochloride, M.P. 147°-149° C., the desired product was obtained, M.P. 192°-195° C.

출처 및 근거

ORD 기록
ord-af5c30c11ada428ab846ec67308168b5
출처 데이터셋
uspto-grants-1979_05
특허 번호
US04153235

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