Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Mesityl oxide → 2,8-Dimethylnona-2,7-dien-4-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Mesityl oxide | HCID 8858 | — |
| 반응물 | 1-Chloro-3-methyl-2-butene | HCID 10429 | — |
| 반응물 | Diacetone Alcohol | HCID 31256 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 2,8-Dimethylnona-2,7-dien-4-one | HCID 13244984 | — |
반응 단계
Acetone under the reaction conditions forms also some diacetone alcohol and mesityl oxide, and these then react with the prenyl chloride to produce the above isomers of prenyl mesityl oxide, also called prenyl-substituted methyl pentenones, in the same manner as acetone reacts with prenyl chloride to produce methyl heptenone. It is also possible that prenyl chloride reacts with the diacetone alcohol in the same manner to give the corresponding hydroxy derivatives that subsequently dehydrate. The presence of such hydroxy ketones is observed in the residues of the methyl heptenone production by the process of U.S. Pat. No. 3,668,255.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04153633 |
| 출처 데이터셋 | uspto-grants-1979_05 |
| ORD ID | ord-5236353093b34b51b46c7a3bb94a86ea |
| 출처 메모 | uspto-grants-1979_05 |