Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Cyano-2-ethoxy-2-methylaminoethylene → HCID 178483853, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Cyano-2-ethoxy-2-methylaminoethylene | HCID 73683202 | — |
| 반응물 | HCID 178433288 | HCID 178433288 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | HCID 178483853 | HCID 178483853 | — |
반응 단계
4-Methyl-5-[(2-aminoethyl)thiomethyl]imidazole (3.5 g) was added to a solution of 1-cyano-2-ethoxy-2-methylaminoethylene in pyridine (3.1 g) and the solution was stirred for 5 hours at 100°. The product was chromatographed on a column of neutral alumina with elution by chloroform/ethyl acetate (1:1) to give the title compound as a glass.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04153704 |
| 출처 데이터셋 | uspto-grants-1979_05 |
| ORD ID | ord-f361e15054704f7da7f4c14e7d6be3a3 |
| 출처 메모 | uspto-grants-1979_05 |