Ethanol → alpha-p-cyclohexylphenyl-N-p-chlorophenylnitrone

HRID 262232

반응식

HRID 262232 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][OH:9])=[CH:4][CH:3]=1.[CH:10]1([C:16]2[CH:23]=[CH:22][C:19](C=O)=[CH:18][CH:17]=2)[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1.[CH2:24](O)C>>[CH2:19]1[CH2:18][CH2:17][CH:16]([C:10]([C:15]2[CH:24]=[CH:11][CH:12]=[CH:13][CH:14]=2)=[N+:8]([C:5]2[CH:6]=[CH:7][C:2]([Cl:1])=[CH:3][CH:4]=2)[O-:9])[CH2:23][CH2:22]1

참가 물질

4

반응물 3

HCID 702EthanolHCID 699834-ChlorophenylhydroxylamineHCID 119689p-Cyclohexylbenzaldehyde

생성물 1

HCID 86736527alpha-p-cyclohexylphenyl-N-p-chlorophenylnitrone

실험 절차

p-Chlorophenylhydroxylamine (0.05 moles) was dissolved in warm 95% ethanol (40 cc) and was treated with p-cyclohexylbenzaldehyde (0.05 moles) with vigorous stirring. The solid which formed was collected, washed with 95% ethanol, and was recrystallized from ethanol to give α-p-cyclohexylphenyl-N-p-chlorophenylnitrone.

후처리

  1. customThe solid which formed
  2. customwas collected
  3. washwashed with 95% ethanol
  4. customwas recrystallized from ethanol

출처 및 근거

ORD 기록
ord-2f3c5ff760414f2dad6390e45c68f9d8
출처 데이터셋
uspto-grants-1979_05
특허 번호
US04153722

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