Hexamethylenetetramine → Molybdenum hexamethylenetetramine

HRID 262286

반응식

HRID 262286 반응식
[CH2:1]1[N:6]2[CH2:7][N:8]3[CH2:10][N:4]([CH2:5]2)[CH2:3][N:2]1[CH2:9]3.O[Mo:12](O)(=O)=O.[NH4+].[NH4+].[O-][Mo]([O-])(=O)=O>O>[Mo:12].[CH2:1]1[N:6]2[CH2:7][N:8]3[CH2:10][N:4]([CH2:5]2)[CH2:3][N:2]1[CH2:9]3

참가 물질

5

반응물 3

HCID 4101HexamethylenetetramineHCID 61578Diammonium molybdateHCID 82208Molybdic acid

생성물 1

HCID 131710930Molybdenum hexamethylenetetramine

시약·촉매·용매 1

HCID 962Water용매2회

실험 절차

Hexamethylenetetramine molybdate having a 2/1 molybdenum/hexamethylenetetramine molar ratio was prepared as follows. 10 grams of hexamethylenetetramine was dissolved in 100 ml water heated near reflux temperature. 24.01 grams of commercial, so-called "molybdic acid" (actually at least one ammonium molybdate) was dissolved in 169 ml water heated to reflux temperature. The first solution was added to the second solution.

후처리

  1. temperatureheated
  2. temperaturenear reflux temperature
  3. temperatureheated
  4. temperatureto reflux temperature
  5. additionThe first solution was added to the second solution

출처 및 근거

ORD 기록
ord-20c3308774ac484e80a640ce77da877a
출처 데이터셋
uspto-grants-1979_05
특허 번호
US04153792

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