4-Diisopropylamino-2-phenyl-butyronitrile → alpha,alpha-Bis[2-(diisopropylamino)ethyl]-alpha-(2-pyridyl)acetonitrile

HRID 262320

반응식

HRID 262320 반응식
[CH:1]([N:4]([CH:16]([CH3:18])[CH3:17])[CH2:5][CH2:6][CH:7]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][N:11]=1)[C:8]#[N:9])([CH3:3])[CH3:2].[CH:19]([N:22]([CH:34]([CH3:36])[CH3:35])[CH2:23][CH2:24]C(C1C=CC=CC=1)C#N)([CH3:21])[CH3:20]>>[CH:16]([N:4]([CH:1]([CH3:3])[CH3:2])[CH2:5][CH2:6][C:7]([CH2:24][CH2:23][N:22]([CH:34]([CH3:36])[CH3:35])[CH:19]([CH3:21])[CH3:20])([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][N:11]=1)[C:8]#[N:9])([CH3:18])[CH3:17]

참가 물질

3

반응물 2

HCID 126122104-Diisopropylamino-2-phenyl-butyronitrileHCID 133196744-Diisopropylamino 2-(2-pyridyl)butyronitrile

생성물 1

HCID 21320525alpha,alpha-Bis[2-(diisopropylamino)ethyl]-alpha-(2-pyridyl)acetonitrile

실험 절차

Substitution of an equivalent quantity of the preceding acetonitrile for α-[2-(diisopropylamino)ethyl]-α-phenylacetonitrile called for in Example 2, Method B and substantial repetition of the procedure detailed in that example, affords α,α-bis[2-(diisopropylamino)ethyl]-α-(2-pyridyl)acetonitrile, as an oil boiling at about 155°-160° C. at 0.3 mm. pressure.

출처 및 근거

ORD 기록
ord-a6e69cff00264bffadfcde88ffed5e31
출처 데이터셋
uspto-grants-1979_05
특허 번호
US04153797

연결된 노트

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