Methylamine → HCID 70510436, 화합물
반응식
CS[C:3]([NH:8][CH2:9][CH2:10][S:11][CH2:12][C:13]1[C:18]([O:19][CH3:20])=[CH:17][CH:16]=[CH:15][N:14]=1)=[CH:4][N+:5]([O-:7])=[O:6].[CH3:21][NH2:22]>C(O)C>[CH3:21][NH:22][C:3]([NH:8][CH2:9][CH2:10][S:11][CH2:12][C:13]1[C:18]([O:19][CH3:20])=[CH:17][CH:16]=[CH:15][N:14]=1)=[CH:4][N+:5]([O-:7])=[O:6]참가 물질
4
실험 절차
1-Methylthio-1-[2-((3-methoxy-2-pyridyl)methylthio)ethylamino]-2-nitroethylene (1.4 g) was stirred with a solution of methylamine in ethanol (25 ml, 33% solution) and dissolved within a minute. After a further 3 minutes a crystalline product separated and recrystallisation from ethanol/ether yielded the title product (1.1 g), m.p. 145.5°-147°.
후처리
- dissolutiondissolved within a minute
- customAfter a further 3 minutes a crystalline product separated
- customrecrystallisation from ethanol/ether
출처 및 근거
- ORD 기록
- ord-e7a577b27ae74f77918edaebe56430ab
- 출처 데이터셋
- uspto-grants-1979_05
- 특허 번호
- US04154838
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