Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → rac-(1R,2R)-2-(dimethylamino)cyclohexan-1-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Dimethylamine | HCID 674 | — |
| 반응물 | Cyclohexene oxide | HCID 9246 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | rac-(1R,2R)-2-(dimethylamino)cyclohexan-1-ol | HCID 15560793 | — |
반응 단계
This compound was previously prepared from cyclohexene oxide and dimethylamine in benzene at room temperature for 14 days in 95% yield, b.p. 90° (20 mm): J. Chem. Soc., 4835 (1965); or in autoclave: C. A. 67, 63899 d, Rocz. Chem. 41, 541 (1967) b.p. 88° (14 mm); also Bull. Soc. Chim. France, 850 (1947): hydrochloride and resolution reported.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04148914 |
| 출처 데이터셋 | uspto-grants-1979_04 |
| ORD ID | ord-89c4a44e39b04448b933484d36cfabda |
| 출처 메모 | uspto-grants-1979_04 |