Ammonia → N-methyldihydrophenethylamine

HRID 26264

반응식

HRID 26264 반응식
[CH3:1][NH:2][CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.[Li].N>C(O)C>[CH3:1][NH:2][CH2:3][CH2:4][CH:5]1[CH:6]=[CH:7][CH:8]=[CH:9][CH2:10]1

참가 물질

5

반응물 3

HCID 222AmmoniaHCID 11503N-MethylbenzeneethanamineHCID 3028194Lithium

생성물 1

HCID 21325368N-methyldihydrophenethylamine

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

46 g. (0.34 moles) of N-methylphenethylamine are reduced by treatment with 16 g. of lithium (2.3 g. atom) in 1.5 l. of ammonia and 250 ml. ethanol according to the procedure of Example 1(a) to yield crude N-methyldihydrophenethylamine.

출처 및 근거

ORD 기록
ord-62363256f8234758ae7a253104fc17bb
출처 데이터셋
uspto-grants-1979_04
특허 번호
US04149001

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