HCID 13290642, 화합물 → 5-Benzyl-4-hydroxymethyloxazole
반응식
[CH2:1]([C:8]1[O:12][CH:11]=[N:10][C:9]=1[C:13](OC)=[O:14])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>O1CCCC1>[CH2:1]([C:8]1[O:12][CH:11]=[N:10][C:9]=1[CH2:13][OH:14])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1참가 물질
4
실험 절차
Methyl 5-benzyl-4-oxazolecarboxylate is reduced with lithium aluminium hydride in tetrahydrofuran to give 5-benzyl-4-hydroxymethyloxazole, which by reacting with thionyl chloride is converted to 5-benzyl-4-chloromethyloxazole.
출처 및 근거
- ORD 기록
- ord-a01f62e16d3b48d6affa01a9ceaa5aaa
- 출처 데이터셋
- uspto-grants-1979_05
- 특허 번호
- US04154844
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