Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,6-Dimethylbenzaldehyde → 1-(2,6-Dimethylbenzylideneamino)-3-(4-pyridylmethyl)guanidine hydriodide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,6-Dimethylbenzaldehyde | HCID 583841 | — |
| 반응물 | HCID 178506606 | HCID 178506606 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 1-(2,6-Dimethylbenzylideneamino)-3-(4-pyridylmethyl)guanidine hydriodide | HCID 178424786 | — |
반응 단계
A mixture of 2.93 g. of 1-amino-3-(4-pyridylmethyl)guanidine hydriodide and 1.34 g. of 2,6-dimethylbenzaldehyde in 5 ml. of glacial acetic acid is heated at 100° C. After 2 hours the solidified reaction mixture is triturated with water and filtered. Crystallization from absolute ethanol gives the desired product as colorless granular crystals, m.p. 197°-200° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04154947 |
| 출처 데이터셋 | uspto-grants-1979_05 |
| ORD ID | ord-6daa0316320243bdb983651b3732a119 |
| 출처 메모 | uspto-grants-1979_05 |