참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | O-Cresol | HCID 335 | — |
| 반응물 | N,N'-Dimethylurea | HCID 7293 | — |
| 반응물 | Maleic acid anilide | HCID 1550938 | — |
| 생성물 | 1,3-Dimethyl-5-(phenylaminocarbonyl methylene)-hydantoin | HCID 54089272 | — |
반응 단계
A mixture of 19.1 parts of N-phenyl maleic acid monoamide 8.8 parts of N,N'-dimethyl urea and 100 parts of cresol is stirred for 2.5 hours at 165° C. The solvent is distilled off in vacuo and the residue fractionated. An oily liquid distills over at a boiling point of from 220° to 223° C./0.1 Torr and solidifies after a while. Recrystallisation from n-propanol gives the compound confirmed by IR- (bands characteristic of hydantoins at 1705 and 1765 cm-1 and of amide at 1690 cm-1) and NMR-spectra.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04156074 |
|---|
| 출처 데이터셋 | uspto-grants-1979_05 |
|---|
| ORD ID | ord-0aac9f2dd7fc4702b97da29a8053b702 |
|---|
| 출처 메모 | uspto-grants-1979_05 |
|---|
