Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenethylamine → N-[[3-Methoxy-2-[3-(4-morpholinyl)propoxy]phenyl]methylene]benzeneethanamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenethylamine | HCID 1001 | — |
| 반응물 | 3-Methoxy-2-[3-(4-morpholinyl)propoxy]benzaldehyde | HCID 2200348 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N-[[3-Methoxy-2-[3-(4-morpholinyl)propoxy]phenyl]methylene]benzeneethanamine | HCID 20298672 | 85.9% |
반응 단계
3-Methoxy-2-[3-(4-morpholinyl)propoxy]benzaldehyde (42.5 g) and 18.5 g of phenethylamine are reacted in 150 ml of toluene following the procedure described in Example 1B, yielding 50.0 g of the title compound, boiling point 229°-234° C. at 0.2-0.3 mm of Hg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04156079 |
| 출처 데이터셋 | uspto-grants-1979_05 |
| ORD ID | ord-7570d6d9087a47b5a8672c3631e77cdd |
| 출처 메모 | uspto-grants-1979_05 |