참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Propionitrile | HCID 7854 | — |
| 반응물 | 2-Octanone | HCID 8093 | — |
| 반응물 | Tetramethylammonium hydroxide | HCID 60966 | — |
| 반응물 | Calciumoxide | HCID 6850728 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-Nonenenitrile, 2,3-dimethyl- | HCID 103749 | — |
반응 단계
Into a 100 ml. flask, equipped with a magnetic stirrer, thermometer, condensor, and static nitrogen head, was placed 13.6 g. of 2-octanone, 11 g. of propionitrile, 61 g. of calcium oxide and 0.3 g. of 25% tetramethyl ammonium hydroxide in water. The mixture was held at reflux (103° C.) for 16 hours at which time gas chromatographic analysis showed 7% product nitrile relative to starting ketone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04156690 |
|---|
| 출처 데이터셋 | uspto-grants-1979_05 |
|---|
| ORD ID | ord-526caeda957f4c6ca162f39a48ff715a |
|---|
| 출처 메모 | uspto-grants-1979_05 |
|---|
