Acrylonitrile → 3-[(3-Hydroxypropyl)amino]propanenitrile

HRID 263172노트

반응식

HRID 263172 반응식
[NH2:1][CH2:2][CH2:3][CH2:4][OH:5].[C:6](#[N:9])[CH:7]=[CH2:8]>>[C:6]([CH2:7][CH2:8][NH:1][CH2:2][CH2:3][CH2:4][OH:5])#[N:9]

참가 물질

3

반응물 2

HCID 7855AcrylonitrileHCID 90863-Amino-1-propanol

생성물 1

HCID 135569403-[(3-Hydroxypropyl)amino]propanenitrile

실험 절차

A solution of 75 g. (1 mole) of 3-aminopropanol is stirred while 54 g. (1 mole) of acrylonitrile is added dropwise. After being allowed to stand at room temperature for several hours and preferably overnight, the reaction mixture is concentrated under reduced pressure at 50° yielding 3-(2-cyanoethyl)aminopropanol.

후처리

  1. concentrationthe reaction mixture is concentrated under reduced pressure at 50°

출처 및 근거

ORD 기록
ord-6c18ed7a1465480899fe070bc71a7c5b
출처 데이터셋
uspto-grants-1979_05
특허 번호
US04156693

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