Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,2-Benzenedicarbonitrile, 4-nitro- → 4-Phenoxyphthalonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,2-Benzenedicarbonitrile, 4-nitro- | HCID 97443 | — |
| 반응물 | Phenolate Sodium | HCID 4445035 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 4-Phenoxyphthalonitrile | HCID 371800 | 49% |
반응 단계
The procedure of Example 35 was followed except that 1,2-dicyano-4-nitrobenzene (1.0 part) was used in place of the 1,2-dicyano-3-nitrobenzene, 1.0 parts instead of 2.79 parts of sodium phenoxide and 20 parts instead of 50 parts of dimethylformamide were used. 1,2-Dicyano-4-phenoxybenzene (0.6 parts, 49%) was obtained as a white solid, m.pt.98°-100° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05730759 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-690d3f8480e44e9f98c5d08baf524723 |
| 출처 메모 | uspto-grants-1998_03 |