Dibutylcarbamoyl chloride → 1,1-Dibutyl-3-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)urea

HRID 263201

반응식

HRID 263201 반응식
[CH2:1]([N:5]([CH2:9][CH2:10][CH2:11][CH3:12])[C:6](Cl)=[O:7])[CH2:2][CH2:3][CH3:4].[S:13]1[CH:17]=[CH:16][C:15]2[CH:18]([NH2:22])[CH2:19][CH2:20][CH2:21][C:14]1=2>>[CH2:1]([N:5]([CH2:9][CH2:10][CH2:11][CH3:12])[C:6]([NH:22][CH:18]1[C:15]2[CH:16]=[CH:17][S:13][C:14]=2[CH2:21][CH2:20][CH2:19]1)=[O:7])[CH2:2][CH2:3][CH3:4]

참가 물질

3

반응물 2

HCID 83371Dibutylcarbamoyl chlorideHCID 42163724,5,6,7-Tetrahydro-1-benzothiophen-4-amine

생성물 1

HCID 203489471,1-Dibutyl-3-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)urea

실험 절차

Similarly, diethyl-, dipropyl-, and dibutylcarbamoyl chloride are reacted with 4,5,6,7-tetrahydrobenzo[b]thiophen-4-amine to afford 1,1-diethyl-, 1,1-dipropyl-, and 1,1-dibutyl-3-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)urea, respectively. Substitution of the above-mentioned carbamoyl chlorides with the corresponding thiocarbamoyl chlorides affords the corresponding thioureas.

출처 및 근거

ORD 기록
ord-d56ba2bfd3fe4bda96e1a5315a80bbcd
출처 데이터셋
uspto-grants-1979_05
특허 번호
US04156670

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