Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Methylbenzo[b]thiophene → 2-(4-Chloro-3-sulfamoylbenzoyl)-3-methyl-benzo[b]thiophene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Methylbenzo[b]thiophene | HCID 73817 | — |
| 반응물 | 3-(Aminosulfonyl)-4-chlorobenzoyl chloride | HCID 3017979 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 용매 | Chlorobenzene | HCID 7964 | — |
| 생성물 | 2-(4-Chloro-3-sulfamoylbenzoyl)-3-methyl-benzo[b]thiophene | HCID 21316639 | — |
반응 단계
is obtained as described in Example 1 from 2.5 g 4-chloro-3-sulfamoylbenzoyl chloride, 1.6 g 3-methylbenzo[b]thiophene and 3 g aluminum chloride in 50 ml chlorobenzene. Colorless crystals, m.p. 210° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04156732 |
| 출처 데이터셋 | uspto-grants-1979_05 |
| ORD ID | ord-c924855fb6344a32ab7dcacaf651a47f |
| 출처 메모 | uspto-grants-1979_05 |