Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Urea → Heptadecyl carbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Urea | HCID 1176 | — |
| 반응물 | 1-Heptadecanol | HCID 15076 | — |
| 촉매 | Nickel | HCID 935 | — |
| 생성물 | Heptadecyl carbamate | HCID 19372549 | 94% |
반응 단계
A mixture of 256 parts of heptadecyl alcohol, 60 parts of urea and 5 parts of a cation exchanger which is commercially available under the registered name Amberlite 200 and, having been treated in accordance with Example 1, contains nickel, is heated in a stirred vessel to 140°-145° C., whilst stirring. After filtering off the exchanger whilst the reaction solution is hot, 280 parts of heptadecyl carbamate are obtained. This corresponds to a yield of 94% of theory. The product has a melting point of 53°-54° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04156784 |
| 출처 데이터셋 | uspto-grants-1979_05 |
| ORD ID | ord-fe91ab106e5b4d84b4b3f5742e1a10df |
| 출처 메모 | uspto-grants-1979_05 |