참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 2-Amino-5-nitropyridine | HCID 77888 | — |
| 생성물 | HCID 178526703 | HCID 178526703 | 60% |
반응 단계
A mixture containing 500 g (3.6 mol) of 2-amino-5-nitropyridine in 2000 ml of 10% sodium hydroxide was refluxed at about 102° C. for 10 hours, cooled and filtered. The filter cake was dissolved in water and neutralized with hydrochloric acid. The product was filtered and dried to give 301.7 g (60%) of product as a white powdery solid, m.p. 188°-190° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04149872 |
|---|
| 출처 데이터셋 | uspto-grants-1979_04 |
|---|
| ORD ID | ord-6ae7801ecbfb4c0cae743ecb62ed22a2 |
|---|
| 출처 메모 | uspto-grants-1979_04 |
|---|
