Methylisothiazolinone → bis-(2-methyl-3-isothiazolone) zinc(II)chloride
반응식
[Cl-:1].[Zn+2:2].[Cl-].[CH3:4][N:5]1[C:9](=[O:10])[CH:8]=[CH:7][S:6]1>C(O)C>[Cl-:1].[Zn+2:2].[CH3:4][N:5]1[C:9](=[O:10])[CH:8]=[CH:7][S:6]1.[CH3:4][N:5]1[C:9](=[O:10])[CH:8]=[CH:7][S:6]1.[Cl-:1]참가 물질
4
실험 절차
To a solution of 3.4 g (0.02 mole) of anhydrous zinc chloride in 130 ml absolute ethanol was added a solution of 2-methyl-3-isothiazolone in 20 ml of absolute ethanol. The clear solution was stirred at room temperature for 30 minutes. Concentration yielded a tan solid. The solid was triturated with ether, filtered, and dried to yield 8.4 g (92%) of bis-(2-methyl-3-isothiazolone) zinc(II)chloride, m.p. 148°-151° C.
후처리
- concentrationConcentration
- customyielded a tan solid
- customThe solid was triturated with ether
- filtrationfiltered
- customdried
출처 및 근거
- ORD 기록
- ord-79a8c7ae42cd4bc490ff92b922e243f9
- 출처 데이터셋
- uspto-grants-1979_04
- 특허 번호
- US04150026
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