Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Nitrobenzyl chloride → 4-Nitrobenzyltriphenylphosphonium chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Nitrobenzyl chloride | HCID 7482 | — |
| 반응물 | Triphenylphosphine | HCID 11776 | — |
| 생성물 | 4-Nitrobenzyltriphenylphosphonium chloride | HCID 12000315 | — |
반응 단계
A solution of 26.3 g (0.10 moles) of triphenylphosphide and 17.2 g (0.10 moles) of p-nitrobenzyl chloride in 50 ml of benezene is refluxed for 2 hours. After cooling the solid is collected and washed with benzene. Crystallization from carbon tetrachloride petroleum ether gives colorless crystals, m.p. 278°-280° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04150105 |
| 출처 데이터셋 | uspto-grants-1979_04 |
| ORD ID | ord-6e5bd4e07c044528b4ceaa1ba598509a |
| 출처 메모 | uspto-grants-1979_04 |