Ethyl bromoacetate → ethyl 5-dodecyl-2H-tetrazole-2-acetate

HRID 264066

반응식

[CH2:1]([C:13]1[NH:17][N:16]=[N:15][N:14]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].C(C1NN=NN=1)CCCCCCCCC.Br[CH2:34][C:35]([O:37][CH2:38][CH3:39])=[O:36].BrC1C=CC=CC=1CC(OCC)=O>>[CH2:1]([C:13]1[N:14]=[N:15][N:16]([CH2:34][C:35]([O:37][CH2:38][CH3:39])=[O:36])[N:17]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

참가 물질

반응물 4

HCID 7748Ethyl bromoacetate

HCID 2780092Ethyl 2-(2-bromophenyl)acetate

HCID 178442802HCID 178442802, 화합물

HCID 178442834HCID 178442834, 화합물

생성물 1

HCID 10782253ethyl 5-dodecyl-2H-tetrazole-2-acetate

실험 절차

When in the general procedure of Example 71 an appropriate amount of 5-dodecyl-1H-tetrazole was substituted for 5-decyl-1H-tetrazole and an appropriate amount of ethyl bromoacetate was substituted for ethyl 2-bromophenylacetate, the title compound was obtained, mp 38°-40° C.

출처 및 근거

ORD 기록: ord-ffc20fdd5b544423afabaf4e2ad082bb
출처 데이터셋: uspto-grants-1997_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05646170

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