Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phosphorus sulfide (P2S5) → Tetradecanethioamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phosphorus sulfide (P2S5) | HCID 14817 | — |
| 반응물 | Tetradecanamide | HCID 69492 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | Tetradecanethioamide | HCID 21469509 | 105.6% |
반응 단계
Phosphorus pentasulfide (9.8 g, 0.044 mol) was added to a mixture of tetradecanamide (8.6 g, 0.04 mol) in dry THF (250 mL) and the mixture refluxed overnight, concentrated in vacuo, and heated with methanol (200 mL), filtered, and the filtrate concentrated in vacuo to yield a pale yellow solid (10.28 g, 99%) used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05646170 |
| 출처 데이터셋 | uspto-grants-1997_07 |
| ORD ID | ord-4ff015936dad43c28e0d560ebd8cf89e |
| 출처 메모 | uspto-grants-1997_07 |