Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl Gentisate → Methyl 5-(3,5,5-trimethylhexyloxy)-2-hydroxybenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl Gentisate | HCID 75077 | — |
| 반응물 | 3,5,5-Trimethylhexyl p-toluenesulfonate | HCID 19036683 | — |
| 생성물 | Methyl 5-(3,5,5-trimethylhexyloxy)-2-hydroxybenzoate | HCID 19036700 | 76% |
반응 단계
Synthesis was carried out in the same manner as in Example 1, except for replacing methyl 2,4-dihydroxybenzoate with methyl 2,5-dihydroxybenzoate and replacing 2-ethylhexyl bromide with 3,5,5-trimethylhexyl p-toluenesulfonate, to obtain methyl 5-(3,5,5-trimethylhexyloxy)-2-hydroxybenzoate represented by the following chemical formula (hereinafter referred to as compound 10) as a colorless, clear and oily substance in a yield of 76%. The analytical results are shown below. ##STR31##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05646184 |
| 출처 데이터셋 | uspto-grants-1997_07 |
| ORD ID | ord-2fd0cb85959e4ba889eb5e6891fecc2f |
| 출처 메모 | uspto-grants-1997_07 |