1-Bromo-2-methylbutane, (+)- → HCID 178418444, 화합물

HRID 2652

반응식

HRID 2652 반응식
Br[CH2:2][C@@H:3]([CH3:6])[CH2:4][CH3:5].FC(F)(F)S(O[C:13]1[CH:18]=[CH:17][C:16]([C@H:19]2[CH2:24][CH2:23][C@H:22]([CH:25]3[CH2:30][CH2:29][Si:28]([CH2:37][CH2:38][CH2:39][CH2:40][CH3:41])(C4C=CC=CC=4)[CH2:27][CH2:26]3)[CH2:21][CH2:20]2)=[CH:15][CH:14]=1)(=O)=O>>[CH2:37]([Si@H:28]1[CH2:27][CH2:26][C@H:25]([C@H:22]2[CH2:21][CH2:20][C@H:19]([C:16]3[CH:15]=[CH:14][C:13]([CH2:2][C@@H:3]([CH3:6])[CH2:4][CH3:5])=[CH:18][CH:17]=3)[CH2:24][CH2:23]2)[CH2:30][CH2:29]1)[CH2:38][CH2:39][CH2:40][CH3:41]

참가 물질

3

반응물 2

HCID 54641671-Bromo-2-methylbutane, (+)-HCID 178418356HCID 178418356, 화합물

생성물 1

HCID 178418444HCID 178418444, 화합물

실험 절차

The general procedure of Example 18 was repeated using (S)-1-bromo-2-methylbutane and (4-(trans-4-(4-n-pentyl-4-phenyl-4-silacyclohexyl)cyclohexyl)phenyl) trifluoromethanesulfonate, thereby obtaining the intended compound.

후처리

  1. customobtaining the intended compound

출처 및 근거

ORD 기록
ord-dd9da67525c44e2d8824e7d3320b62e1
출처 데이터셋
uspto-grants-1998_03
특허 번호
US05730902

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