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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 265208생성일: 2026년 10월 25일

Azobisisobutyronitrile → 3,6-Dimethyl-3-octanol

https://huagongshe.com/reaction/265208

반응식

참여 물질

역할이름HCID투입량
반응물AzobisisobutyronitrileHCID 6547—
반응물Methyl AcrylateHCID 7294—
반응물Benzyl methacrylateHCID 17236—
반응물Methyl 3-mercaptopropionateHCID 18050—
반응물2-MethyldecaneHCID 23415—
생성물3,6-Dimethyl-3-octanolHCID 9027—

반응 조건

온도60 °C

반응 단계

A mixed solution of the whole amount of the above-described resin grain dispersion (as seed) and 10 g of Dispersion Stabilizing Resin (Q-1) was heated to a temperature of 60° C. under nitrogen gas stream with stirring. To the mixture was added dropwise a mixture of 85 g of benzyl methacrylate, 15 g of methyl acrylate, 1.0 g of methyl 3-mercaptopropionate, 0.8 g of AIVN and 200 g of Isopar H over a period of 2 hours, followed by further reacting for 2 hours. Then 0.8 g of AIVN was added to the reaction mixture, the temperature thereof was raised to 70° C., and the reaction was conducted for 2 hours. Further, 0.6 g of AIVN was added thereto, followed by reacting for 3 hours. After cooling, the reaction mixture was passed through a nylon cloth of 200 mesh to obtain a white dispersion which was a latex of good monodispersity having a polymerization ratio of 98% and an average grain diameter of 0.25 μm.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05648190
출처 데이터셋uspto-grants-1997_07
ORD IDord-ae589cc75aba45d6af1a9ea5840a6d3b
출처 메모uspto-grants-1997_07