Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
m-Chloroperbenzoic acid → 11-methylene-3-methylsulfinyl-11H-s-triazolo[3,4-b][3]benzazepine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | m-Chloroperbenzoic acid | HCID 70297 | — |
| 반응물 | 11-methylene-3-methylthio-11H-s-triazolo[3,4-b][3]benzazepine | HCID 21323409 | — |
| 생성물 | 11-methylene-3-methylsulfinyl-11H-s-triazolo[3,4-b][3]benzazepine | HCID 21323367 | — |
반응 단계
By a procedure similar to that of Example 17, the reaction of 11-methylene-3-methylthio-11H-s-triazolo[3,4-b][3]benzazepine with m-chloroperbenzoic acid gave 11-methylene-3-methylsulfinyl-11H-s-triazolo[3,4-b][3]benzazepine as crystals. Recrystallization from ethyl acetate yielded colorless prisms, m.p. 140°-142° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04150139 |
| 출처 데이터셋 | uspto-grants-1979_04 |
| ORD ID | ord-9ffaacf5506e43fda0f716845647efb3 |
| 출처 메모 | uspto-grants-1979_04 |