반응식
[CH2:1]=[C:2]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=2[CH:6]=[CH:5][N:4]2[C:13]([S:16][CH3:17])=[N:14][N:15]=[C:3]12.ClC1C=CC=C(C(OO)=[O:26])C=1>>[CH2:1]=[C:2]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=2[CH:6]=[CH:5][N:4]2[C:13]([S:16]([CH3:17])=[O:26])=[N:14][N:15]=[C:3]12참가 물질
3
실험 절차
By a procedure similar to that of Example 17, the reaction of 11-methylene-3-methylthio-11H-s-triazolo[3,4-b][3]benzazepine with m-chloroperbenzoic acid gave 11-methylene-3-methylsulfinyl-11H-s-triazolo[3,4-b][3]benzazepine as crystals. Recrystallization from ethyl acetate yielded colorless prisms, m.p. 140°-142° C.
출처 및 근거
- ORD 기록
- ord-9ffaacf5506e43fda0f716845647efb3
- 출처 데이터셋
- uspto-grants-1979_04
- 특허 번호
- US04150139
연결된 노트
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