Sodium Methoxide → 3-methoxy-11-phenyl-11H-s-triazolo[3,4-b][3]benzazepine

HRID 26531노트

반응식

HRID 26531 반응식
CS([C:5]1[N:14]2[C:8]([CH:9]([C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[C:10]3[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=3[CH:12]=[CH:13]2)=[N:7][N:6]=1)(=O)=O.[CH3:25][O-:26].[Na+]>>[CH3:25][O:26][C:5]1[N:14]2[C:8]([CH:9]([C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[C:10]3[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=3[CH:12]=[CH:13]2)=[N:7][N:6]=1

참가 물질

3

반응물 2

HCID 10942334Sodium MethoxideHCID 213233363-methylsulfonyl-11-phenyl-11H-s-triazolo[3,4-b][3]benzazepine

생성물 1

HCID 213233983-methoxy-11-phenyl-11H-s-triazolo[3,4-b][3]benzazepine

실험 절차

The reaction of 3-methylsulfonyl-11-phenyl-11H-s-triazolo[3,4-b][3]benzazepine with sodium methoxide yielded 3-methoxy-11-phenyl-11H-s-triazolo[3,4-b][3]benzazepine. Colorless prisms (as recrystallized from aqueous methanol), melting point: 183°-184° C.

출처 및 근거

ORD 기록
ord-ee7069382bb34b7aa90aeb4921fb8a59
출처 데이터셋
uspto-grants-1979_04
특허 번호
US04150139

반응 노트

불러오는 중…