반응식
[CH2:1]=[C:2]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=2[CH:6]=[CH:5][N:4]2[C:13](S(C)=O)=[N:14][N:15]=[C:3]12.[CH3:19][O-:20].[Na+]>>[CH3:19][O:20][C:13]1[N:4]2[C:3]([C:2](=[CH2:1])[C:8]3[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=3[CH:6]=[CH:5]2)=[N:15][N:14]=1참가 물질
3
실험 절차
The reaction of 11-methylene-3-methylsulfinyl-11H-s-triazolo[3,4-b][3]benzazepine with sodium methoxide yielded 3-methoxy-11-methylene-11H-s-triazolo[3,4-b][3]benzazepine. Colorless needles (as recrystallized from ethyl acetate), melting point: 160°-161° C.
출처 및 근거
- ORD 기록
- ord-9fe685a61e1441ed99838e6823645101
- 출처 데이터셋
- uspto-grants-1979_04
- 특허 번호
- US04150139
연결된 노트
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