Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → 7-(3,4,5-Triphenyl-2-oxo-2,3-dihydroimidazol-1-yl)heptanonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Heptanenitrile, 7-bromo- | HCID 88737 | — |
| 반응물 | 1,4,5-Triphenyl-1,3-dihydro-2H-imidazol-2-one | HCID 628544 | — |
| 용매 | Methyl Ethyl Ketone | HCID 6569 | — |
| 생성물 | 7-(3,4,5-Triphenyl-2-oxo-2,3-dihydroimidazol-1-yl)heptanonitrile | HCID 22916372 | — |
반응 단계
1,4,5-Triphenylimidazol-2-one was treated with 7-bromo-heptanonitrile and potassium carbonate in butanone to give after chromatographic work-up 7-(3,4,5-triphenyl-2-oxo-2,3-dihydroimidazol-1-yl)heptanonitrile, m.p. 100°-101° C., Found: C, 79.7; H, 6.6; N, 9.8%; C28H27N3O requires: C, 79.9; H, 6.4; N, 10.0%; and
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05648373 |
| 출처 데이터셋 | uspto-grants-1997_07 |
| ORD ID | ord-651a0eb968ab4abe943762bc02b8d73d |
| 출처 메모 | uspto-grants-1997_07 |