Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → 1-(8-Bromooctyl)-4,5-diphenyltriazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 1,8-Dibromooctane | HCID 78310 | — |
| 반응물 | HCID 178420171 | HCID 178420171 | — |
| 용매 | Methyl Ethyl Ketone | HCID 6569 | — |
| 생성물 | 1-(8-Bromooctyl)-4,5-diphenyltriazole | HCID 22916394 | — |
반응 단계
4,5-Diphenyl-1,2,3-triazole was treated with 1,8-dibromooctane and potassium carbonate in butanone to give after chromatographic work up the title compound, m.p. 90°-91° C., Found: C, 64.0; H, 6.5; N, 10.1; Br, 19.8%; C22H26BrN3 requires: C, 64.1;H, 6.4; N, 10.2; Br, 19.4%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05648373 |
| 출처 데이터셋 | uspto-grants-1997_07 |
| ORD ID | ord-12c89d6856e24cfdbb6d901fe40e713f |
| 출처 메모 | uspto-grants-1997_07 |