Potassium Carbonate → HCID 22916432, 화합물

HRID 265414

반응식

HRID 265414 반응식
[C:1]1([C:7]2[N:8]=[N:9][NH:10][C:11]=2[C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Br[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][OH:28].C(=O)([O-])[O-].[K+].[K+]>CC(=O)CC>[OH:28][CH2:27][CH2:26][CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][CH2:20][CH2:19][N:9]1[N:8]=[C:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[C:11]([C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=2)=[N:10]1

참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 1087001-Nonanol, 9-bromo-HCID 178420171HCID 178420171, 화합물

생성물 1

HCID 22916432HCID 22916432, 화합물

시약·촉매·용매 1

HCID 6569Methyl Ethyl Ketone용매

실험 절차

4,5-Diphenyl-1,2,3-triazole was treated with 9-bromononan-1-ol and potassium carbonate in butanone to give after chromatography the title compound as a light brown oil.

출처 및 근거

ORD 기록
ord-408b46237a8846728d28274e95007709
출처 데이터셋
uspto-grants-1997_07
특허 번호
US05648373

연결된 노트

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