Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
11-Bromoundecanoic acid → Undecanoyl chloride, 11-bromo-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 11-Bromoundecanoic acid | HCID 17812 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Undecanoyl chloride, 11-bromo- | HCID 85202 | — |
반응 단계
A solution of 11-bromoundecanoic acid (10.00 g, 37.7 mmol) dissolved in CH2Cl2 (30 mL) was slowly added to a solution of SOCl2 (7.0 mL, 94.0 mmol) in CH2Cl2 (25 mL). The mixture was refluxed for 5 h, then concentrated in vacuo to give 11-bromoundecanoyl chloride, which was used without further purification:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05650101 |
| 출처 데이터셋 | uspto-grants-1997_07 |
| ORD ID | ord-788d43050e674b10870d83acc19291d6 |
| 출처 메모 | uspto-grants-1997_07 |