Dicyclohexylcarbodiimide → 2-Dimethylaminopyridine

HRID 266183

반응식

HRID 266183 반응식
[CH3:1][C@H]1OC(=O)C2C(O)=CC(O)=C(Cl)C=2CC(=O)C=CC=C[C@H]2O[C@H]2C1.C1(CCCCCC(O)=O)C=CC=CC=1.[CH:40]1([N:46]=[C:47]=[N:48][CH:49]2[CH2:54][CH2:53][CH2:52]CC2)CCCCC1>O1CCCC1>[CH3:1][N:46]([C:47]1[CH:52]=[CH:53][CH:54]=[CH:49][N:48]=1)[CH3:40]

참가 물질

5

반응물 3

HCID 10868DicyclohexylcarbodiimideHCID 796956-Phenylhexanoic AcidHCID 11268547CID 11268547

생성물 1

HCID 218852-Dimethylaminopyridine

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

Following a procedure similar to that described in Example 12, but using 500 mg of radicicol, 659 mg of 6-phenylhexanoic acid, 15 ml of dry tetrahydrofuran, 707 mg of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 704 mg of the title compound were obtained.

출처 및 근거

ORD 기록
ord-ee70a8c6142e45f0a8bd72be08f42f20
출처 데이터셋
uspto-grants-1997_07
특허 번호
US05650430

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