Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dicyclohexylcarbodiimide → 2-Dimethylaminopyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 반응물 | 3-Thiophen-2-ylprop-2-enoic acid | HCID 92868 | — |
| 반응물 | CID 11268547 | HCID 11268547 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 2-Dimethylaminopyridine | HCID 21885 | — |
반응 단계
Following a procedure similar to that described in Example 12, but using 365 mg of radicicol, 462 mg of 3-(2-thienyl)acrylic acid, 10 ml of dry tetrahydrofuran, 619 mg of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 526 mg of the title compound were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05650430 |
| 출처 데이터셋 | uspto-grants-1997_07 |
| ORD ID | ord-fea62a5a91c84935a8f513fa5cfaaa54 |
| 출처 메모 | uspto-grants-1997_07 |