Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethyl phosphonoacetate → HCID 178473138, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethyl phosphonoacetate | HCID 13345 | — |
| 반응물 | Phosphorus pentachloride | HCID 24819 | — |
| 반응물 | Ethyl(ethoxychlorophosphinyl)acetate | HCID 12634156 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | HCID 178473138 | HCID 178473138 | — |
반응 단계
Ethyl(diethoxyphosphinyl)acetate (11.2 gm., 0.05 mol.) and phosphorus pentachloride (10.5 gm., 0.05 mol.) are dissolved in 200 ml. of benzene and refluxed overnight. The solvent is removed in vacuo, leaving yellow, oily, ethyl(ethoxychlorophosphinyl)acetate as residue (11.5 gm.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04151172 |
| 출처 데이터셋 | uspto-grants-1979_04 |
| ORD ID | ord-f5f7c881caa9453e8959c0b4ff68e9d8 |
| 출처 메모 | uspto-grants-1979_04 |