Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → Propanoicacid, 3-phosphono-, 1-methyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | 2-Phosphonopropionic acid | HCID 73187 | — |
| 생성물 | Propanoicacid, 3-phosphono-, 1-methyl ester | HCID 18623049 | — |
반응 단계
A solution of 2-phosphonopropionic acid (11.2 g., 0.073 moles) in methanol (150 ml.) is heated at reflux for eighteen hours. The methanol is removed in vacuo. Electrophoresis (0.1 N NH4HCO3, 2000 V, 20 minutes, 7.5 cm) indicates complete conversion to the desired product, methyl 2-phosphonopropionate; yield quantitative.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04151172 |
| 출처 데이터셋 | uspto-grants-1979_04 |
| ORD ID | ord-08ed6c28926644e49ea3dd1c4b37bece |
| 출처 메모 | uspto-grants-1979_04 |