Prop-2-en-1-yl 3-nitrobenzoate → Allyl 3-aminobenzoate

HRID 266842노트

반응식

HRID 266842 반응식
[N+:1]([C:4]1[CH:5]=[C:6]([CH:13]=[CH:14][CH:15]=1)[C:7]([O:9][CH2:10][CH:11]=[CH2:12])=[O:8])([O-])=O>CO>[NH2:1][C:4]1[CH:5]=[C:6]([CH:13]=[CH:14][CH:15]=1)[C:7]([O:9][CH2:10][CH:11]=[CH2:12])=[O:8]

참가 물질

3

반응물 1

HCID 14980143Prop-2-en-1-yl 3-nitrobenzoate

생성물 1

HCID 18930599Allyl 3-aminobenzoate

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Reduction of the above nitro compound by the method of Example 2, except that the solvent was methanol, gave allyl 3-aminobenzoate. Nmr (CDCl3): δ 3.38 (br, 2H); 4.79 (dt, 2H); 5.24-5.44 (m, 2H); 5.93-6.09 (m, 1H); 6.86 (dm, 1H); 7.21 (t, 1H); 7.37 (t, 1H); 7.45 (dt, 1H).

출처 및 근거

ORD 기록
ord-b9fec04720d4418b8f0e0887c89a39c7
출처 데이터셋
uspto-grants-1997_07
특허 번호
US05652233

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