Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Aminoacetaldehyde → 1-[alpha-(o-Chlorophenyl)-o-tolyl]imidazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Aminoacetaldehyde | HCID 363 | — |
| 반응물 | Trimethyl orthoformate | HCID 9005 | — |
| 반응물 | 2-[(2-Chlorophenyl)methyl]aniline | HCID 13426664 | — |
| 촉매 | Titanium Tetrachloride | HCID 24193 | — |
| 용매 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 생성물 | 1-[alpha-(o-Chlorophenyl)-o-tolyl]imidazole | HCID 21497409 | — |
반응 단계
In the manner given in Example 1, α-(0-chlorophenyl)-0-toluidine is reacted first with trimethyl orthoformate; the resulting product is reacted with aminoacetaldehyde, dimethyl acetal, and the resulting product of this reaction is heated with titanium tetrachloride in monoglyme to give 1-[α-(0-chlorophenyl)-0-tolyl]imidazole.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03941802 |
| 출처 데이터셋 | uspto-grants-1976_03 |
| ORD ID | ord-f06bfcfd0f2d436682cbfdbb504b6f16 |
| 출처 메모 | uspto-grants-1976_03 |