반응식
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][C:9]1[C:10](=[CH:12][CH:13]=[CH:14][CH:15]=1)[NH2:11].[CH:16](OC)(OC)OC.[NH2:23][CH2:24][CH:25]=O>C(COC)OC.[Ti](Cl)(Cl)(Cl)Cl>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][C:9]1[CH:15]=[CH:14][CH:13]=[CH:12][C:10]=1[N:11]1[CH:25]=[CH:24][N:23]=[CH:16]1참가 물질
6
실험 절차
In the manner given in Example 1, α-(0-chlorophenyl)-0-toluidine is reacted first with trimethyl orthoformate; the resulting product is reacted with aminoacetaldehyde, dimethyl acetal, and the resulting product of this reaction is heated with titanium tetrachloride in monoglyme to give 1-[α-(0-chlorophenyl)-0-tolyl]imidazole.
출처 및 근거
- ORD 기록
- ord-f06bfcfd0f2d436682cbfdbb504b6f16
- 출처 데이터셋
- uspto-grants-1976_03
- 특허 번호
- US03941802
연결된 노트
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