4-Chlorobenzaldehyde → HCID 178504058, 화합물

HRID 267322노트

반응식

Br[C:2]1[CH:14]=[CH:13][C:5]([CH:6]=[N:7][NH:8][C:9](=[NH:12])[S:10][CH3:11])=[CH:4][CH:3]=1.[Cl:15]C1C=CC(C=O)=CC=1.C(=N)(SC)NN.C(C1C=CC(C=O)=CC=1)#N.I.C(=N)(SCC)NN.Br.[Cl:49]C1C=C(C=CC=1Cl)C=NNC(=N)SCCC.ClC1C=C(C=CC=1Cl)C=O.Br.C(=N)(SCCC)NN>>[ClH:15].[Cl:49][C:2]1[CH:14]=[CH:13][C:5]([CH:6]=[N:7][NH:8][C:9](=[NH:12])[S:10][CH3:11])=[CH:4][CH:3]=1

참가 물질

반응물 8

HCID 77264-Chlorobenzaldehyde

HCID 227103,4-Dichlorobenzaldehyde

HCID 660424-Cyanobenzaldehyde

HCID 178419558HCID 178419558, 화합물

HCID 178419559HCID 178419559, 화합물

HCID 178477489HCID 178477489, 화합물

HCID 178504051Methyl hydrazinecarbimidothioate

HCID 178504057HCID 178504057, 화합물

생성물 1

HCID 178504058HCID 178504058, 화합물

실험 절차

The following are prepared in like manner: methyl 3-(4-bromobenzylidene)thiocarbazimidate methosulfate from 4-chlorobenzaldehyde and methyl thiocarbazimidate methosulfate, ethyl 3-(4-cyanobenzylidine)thiocarbazimidate hydroiodide from 4-cyanobenzaldehyde and ethyl thiocarbazimidate hydroiodide, and propyl 3-(3,4-dichlorobenzylidene)thiocarbazimidate hydrobromide from 3,4-dichlorobenzaldehyde and propyl thiocarbazimidate hydrobromide.

후처리

customThe following are prepared in like manner

출처 및 근거

ORD 기록: ord-02088281e21a43ab8944a99d0e44aef2
출처 데이터셋: uspto-grants-1976_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US03941825

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