Methyl Chloride → HCID 178504058, 화합물

HRID 267323노트

반응식

HRID 267323 반응식
[CH3:1]Cl.[Cl:3][C:4]1[CH:15]=[CH:14][C:7]([CH:8]=[N:9][NH:10][C:11]([NH2:13])=[S:12])=[CH:6][CH:5]=1>C(O)C>[ClH:3].[Cl:3][C:4]1[CH:15]=[CH:14][C:7]([CH:8]=[N:9][NH:10][C:11](=[NH:13])[S:12][CH3:1])=[CH:6][CH:5]=1

참가 물질

4

반응물 2

HCID 6327Methyl ChlorideHCID 6680994-Chlorobenzaldehyde thiosemicarbazone

생성물 1

HCID 178504058HCID 178504058, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A 10% molar excess of methyl chloride is added to 2.14 g. of 4-chlorobenzaldehyde thiosemicarbazone and 25 ml. of a anhydrous ethanol in a pressure vessel. The reaction mixture is magnetically stirred and heated in an oil bath for 11/2 hour. The crystalline title compound separates on cooling and is filtered off and air dried.

후처리

  1. temperatureheated in an oil bath for 11/2 hour

출처 및 근거

ORD 기록
ord-f0cdb51be2cb4997a591ba750bee2d9e
출처 데이터셋
uspto-grants-1976_03
특허 번호
US03941825

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