Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Aminoacetaldehyde → 1-(alpha-Phenyl-o-tolyl)imidazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Aminoacetaldehyde | HCID 363 | — |
| 반응물 | Trimethyl orthoformate | HCID 9005 | — |
| 반응물 | 2-Benzylaniline | HCID 119805 | — |
| 촉매 | Titanium Tetrachloride | HCID 24193 | — |
| 용매 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 생성물 | 1-(alpha-Phenyl-o-tolyl)imidazole | HCID 21497358 | — |
반응 단계
In the manner given in Preparation 21, α-phenyl-o-toluidine is reacted first with trimethyl orthoformate, the resulting product is reacted with aminoacetaldehyde, dimethyl acetal, and the resulting product of this reaction is heated with titanium tetrachloride in monoglyme to give 1-(α-phenyl-o-tolyl)imidazole.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03941803 |
| 출처 데이터셋 | uspto-grants-1976_03 |
| ORD ID | ord-95c6e07595134a3592a956073228a28d |
| 출처 메모 | uspto-grants-1976_03 |