Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Butanol → 2-Hydroxydecyl-butyl ether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Butanol | HCID 263 | — |
| 반응물 | Ethylene Oxide | HCID 6354 | — |
| 반응물 | 1,2-Epoxydecane | HCID 16993 | — |
| 반응물 | Sodium | HCID 5360545 | — |
| 촉매 | Sodium Methoxide | HCID 10942334 | — |
| 생성물 | 2-Hydroxydecyl-butyl ether | HCID 10466415 | — |
반응 단계
As described in Example 1, 1 mol of 1,2-epoxydecane was caused to react with 5 times the molar quantity of n-butanol and 0.04 gm-atom of sodium. After distillation of the excess alcohol, the reaction with 10 mols of ethylene oxide was conducted in an autoclave under the conditions described in Example 1, except for the addition of the sodium methylate catalyst. The product thus obtained had a cloud point of 64°C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03943178 |
| 출처 데이터셋 | uspto-grants-1976_03 |
| ORD ID | ord-5d32d71825f34bd8a73662fac1561a93 |
| 출처 메모 | uspto-grants-1976_03 |