Sodium Iodide → HCID 178502576, 화합물

HRID 267645

반응식

HRID 267645 반응식
[CH3:1][O:2][C:3]([P:5](=[O:12])([O:9][CH2:10][CH3:11])[O:6]CC)=[O:4].[I-].[Na+:14]>O1CCCC1>[CH3:1][O:2][C:3]([P:5](=[O:6])([OH:12])[OH:9])=[O:4].[CH2:10]([Na:14])[CH3:11]

참가 물질

4

반응물 2

HCID 5238Sodium IodideHCID 170573Phosphinecarboxylic acid, 1,1-diethoxy-, methyl ester, 1-oxide

생성물 1

HCID 178502576HCID 178502576, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

A solution of 5.9 parts of diethyl methoxycarbonylphosphonate and 4.5 parts of sodium iodide was stirred at room temperature in 50 parts of tetrahydrofuran for 60 hours. The resulting mixture was filtered to give 3.5 parts of the desired ethyl sodium methoxycarbonylphosphonate, m.p. 123°d.

후처리

  1. filtrationThe resulting mixture was filtered

출처 및 근거

ORD 기록
ord-06455ecc7d1146709419d5a44461d24b
출처 데이터셋
uspto-grants-1976_03
특허 번호
US03943201

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